Volume no :4, Issue no: 1,

THE EFFECT OF DRYING METHODS ON THE TEXTURAL PROPERTIES OF THE PSEUDOBOEHMITE SYNTHESIZED BY HOMOGENEOUS PRECIPITATION

Author's: Adrián Zamorategui, Julio A. Soto and Satoshi Sugita
Pages: [1] - [17]
Received Date: November 25, 2012; Revised December 15, 2012.
Submitted by:

Abstract

Pseudoboehmite was prepared by using basic aluminum sulphate as a raw material, which was synthesized by homogeneous precipitation. This BAS was neutralized in solid/liquid reaction with ammonium hydroxide in order to transform to aluminum hydroxide. The hydroxide was dried by three different routes: spray drying, freeze drying, and oven drying. The effect of the drying methods on the final textural properties of the heat treated pseudoboehmite was evaluated. Spray drying was the best route to obtain high surface area for pseudoboehmite heat treated at 450°C It was better than the obtained by the use of freeze and oven dried routes as indicated by BET analysis (350 and respectively. Homogeneous precipitation offers the possibility to obtain powder with a high specific surface area and fibrous morphology.

Keywords

homogeneous precipitation, pseudoboehmite, spray drying, freeze drying, oven drying.